Development and validation of an analytical method for assessing the authenticity of Vaccinium myrtillus shoots L

Development and validation of an analytical method for assessing the authenticity of Vaccinium myrtillus shoots L

AUTHORS : Mechikovaone G.Ya. | Matyushchenkoone N.V. | Smirnova2 O.V.

RELEVANT UNIVERSITIES : oneFar Eastern State Medical University, Khabarovsk, 2FSBI “IMTSEUAOSMP”
Roszdravnadzor, Moscow
YEAR : 2014

 

SUMMARY A method has been developed for determining the authenticity of common blueberry shoots by chromatography in a thin layer of sorbent. The optimal conditions for chromatographic analysis have been determined. The method was validated according to the following parameters: specificity, precision
and robustness. It was found that all the validation characteristics under study are within the acceptance criteria. The results of validation made it possible to include the developed methodology in the draft of the pharmacopoeial monograph “Common bilberry shoots – whole, crushed and Angro powder,” adopted for
consideration by the FGBU “NTs ESMP” of the Ministry of Health of Russia (input No. 6473 of 23.04.13).

 

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